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Interpretable machine learning and hybrid metaheuristic algorithms for multi-objective optimization in injection molding 注射成型多目标优化的可解释机器学习和混合元启发式算法
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-10-14 DOI: 10.1007/s12289-026-02095-7
Liuyu Zhu, Xiying Fan, Yonghuan Guo, Dazhen Zhu, Zhijiang Wang, Lie Li

Warpage deformation and volumetric shrinkage defects in injection molding significantly affect the quality and service life of plastic products. To address this issue, this study proposes a multi-objective process parameter optimization approach. First, MIC screening was applied to 152 central-composite-design/Moldflow samples, and a GAN generated 48 additional samples, producing a 200-sample modeling dataset. Then, a hybrid framework combining the Kepler Optimization Algorithm (KOA) and Ivy Optimization Algorithm (IVYA) was applied for hyperparameter tuning. Furthermore, the interpretability of the Extreme Gradient Boosting (XGBoost) model was enhanced using Shapley Additive Explanations (SHAP), which also provided refined search ranges for process parameters. Finally, multi-objective chaotic game optimization (MOCGO) was used to identify the Pareto front and select a compromise solution. Compared with the initial settings, the selected solution reduced warpage deformation and volumetric shrinkage by 35.7% and 10.1%, respectively.

注塑成型中的翘曲变形和体积收缩缺陷严重影响塑料制品的质量和使用寿命。针对这一问题,本研究提出了一种多目标工艺参数优化方法。首先,MIC筛选应用于152个中心复合设计/Moldflow样本,GAN生成48个额外样本,生成200个样本的建模数据集。然后,采用Kepler优化算法(KOA)和Ivy优化算法(IVYA)相结合的混合框架进行超参数整定。此外,使用Shapley加性解释(SHAP)增强了极端梯度增强(XGBoost)模型的可解释性,该模型还提供了精细的过程参数搜索范围。最后,利用多目标混沌博弈优化算法(MOCGO)识别Pareto前沿并选择折中解。与初始设置相比,所选溶液的翘曲变形和体积收缩率分别降低了35.7%和10.1%。
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引用次数: 0
Finite element analysis of the response of DP800 steel sheet in a new laboratory forming test DP800钢板在新型实验室成形试验中的响应有限元分析
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-10-13 DOI: 10.1007/s12289-026-02092-w
Rahul Rakshit, Benoit Revil-Baudard, Oana Cazacu

Owing to the good formability combined with low yield-to-ultimate tensile strength ratio, DP800 steel is widely used in the automotive industry. For process optimization and analysis of the feasibility and resulting part quality, it is essential to use a suitable constitutive model. To assess the predictive capabilities of models for forming applications, very recently a benchmark focusing on simulation of a new laboratory forming test, called material under control (MUC) was launched. In this paper, we show that an elastoplastic model with yielding described by the 3-D orthotropic yield criteria of Hill48 [1] and Cazacu [2], and isotropic hardening accurately predict the observed plastic anisotropy of the DP800 steel. The predictive capabilities of these models are demonstrated through comparisons between simulation results and experimental data in uniaxial tension and MUC-Tests, including punch force-displacement curves and surface strain distributions for all specimen geometries. Furthermore, the effect of specimen orientation on the strain path experienced by the material during a MUC test was investigated using Cazacu [2] criterion. The results presented suggest that the use of 3-D orthotropic yield criteria and isotropic hardening may provide reliable virtual assessments of DP800 steel for forming operations.

DP800钢具有良好的成形性能和较低的屈服极限抗拉强度比,在汽车工业中得到了广泛的应用。在工艺优化、可行性分析和零件质量分析中,选择合适的本构模型至关重要。为了评估模型在成形应用中的预测能力,最近推出了一项基准测试,重点是模拟一种新的实验室成形测试,称为材料控制(MUC)。采用Hill48[1]和Cazacu[2]的三维正交各向异性屈服准则和各向同性硬化描述的弹塑性模型准确地预测了DP800钢的塑性各向异性。这些模型的预测能力通过单轴拉伸和muc测试的模拟结果与实验数据的比较得到证明,包括冲床力-位移曲线和所有试样几何形状的表面应变分布。此外,采用Cazacu[2]准则研究了试样取向对材料在MUC试验中经历的应变路径的影响。结果表明,采用三维正交各向异性屈服准则和各向同性硬化可以为DP800钢的成形操作提供可靠的虚拟评估。
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引用次数: 0
Data-efficient surrogate modeling using Laplace-Beltrami shape-features: a case study on a cup drawing process 使用拉普拉斯-贝尔特拉米形状特征的数据高效代理建模:一个杯子绘图过程的案例研究
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-10-09 DOI: 10.1007/s12289-026-02091-x
Daniela Steffes-lai, Lukas Morand, Rodrigo Iza-Teran, Tom Niklas Klein, Dirk Helm, Raoul Heese, Jochen Garcke

Process control and optimization are important aspects of manufacturing processes. Surrogate models, i.e. data driven models obtained from numerical simulations, are often employed to predict the process outcome for given process parameters in real time. In this work, we investigate a Laplace-Beltrami shape-feature approach for constructing a surrogate model for cup drawing process simulations. The resulting surrogate model captures local changes in deformations and field quantities on mesh geometries more accurately than standard methods. However, comparing mesh distortions, especially local mesh qualities, is challenging. To address this, we introduce a measure of improvement of mesh distortion to analyse the obtained error distributions. We demonstrate the benefits of the proposed method in contrast to variance-based methods such as principal component analysis, which do not adequately model local variations.

过程控制和优化是制造过程的重要方面。代理模型,即从数值模拟中获得的数据驱动模型,通常用于实时预测给定工艺参数的工艺结果。在这项工作中,我们研究了一种拉普拉斯-贝尔特拉米形状特征方法,用于构建杯子拉伸过程模拟的代理模型。由此产生的代理模型比标准方法更准确地捕获网格几何形状上变形和场量的局部变化。然而,比较网格变形,特别是局部网格质量,是具有挑战性的。为了解决这个问题,我们引入了一种改进网格畸变的方法来分析得到的误差分布。我们证明了与基于方差的方法(如主成分分析)相比,所提出的方法的好处,这些方法不能充分地模拟局部变化。
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引用次数: 0
Springback suppression in 3D bending-torsion combined forming of hollow rectangular aluminum profiles using magnetorheological elastomer inner support 磁流变弹性体内支撑抑制中空矩形铝型材三维弯扭复合成形中的回弹
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-10-08 DOI: 10.1007/s12289-026-02093-9
Yu Wen, Jicai Liang, Yi Li, Ce Liang

Magnetorheological elastomers (MREs), due to their excellent controllable mechanical properties, have broad application prospects in assisting forming processes. In this study, several MREs with varying carbonyl iron powder (CIP) contents are prepared and used for the three-dimensional bending-torsion combined forming of hollow rectangular 6005 A aluminum profiles. A numerical-analytical (FE-TA) model is established to analyze the springback of the profile. The FE-TA model and numerical simulations are used to investigate the effects of varying CIP content and magnetic field strength on the profile’s springback. The results indicate that adding MRE increases the springback of the profile, with magnetic field strength having a more significant effect on springback than CIP content. The maximum error between the springback amount calculated by the FE-TA model and the value obtained by numerical simulation is only 6.75%. Finally, experiments verified the influence of magnetic field strength on profile springback and the accuracy of the numerical simulation.

磁流变弹性体(MREs)由于其优异的可控力学性能,在辅助成形工艺方面有着广阔的应用前景。本研究制备了几种不同羰基铁粉(CIP)含量的MREs,并将其用于中空矩形6005a铝型材的三维弯曲-扭转复合成形。建立了一种数值解析(FE-TA)模型来分析型材的回弹。利用FE-TA模型和数值模拟研究了不同CIP含量和磁场强度对型材回弹的影响。结果表明:MRE的加入提高了型材的回弹率,且磁场强度对回弹率的影响比CIP含量更显著。FE-TA模型计算的回弹量与数值模拟结果的最大误差仅为6.75%。最后,通过实验验证了磁场强度对型材回弹的影响以及数值模拟的准确性。
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引用次数: 0
Achieving strength-ductility synergy in As-cast 7075 aluminum alloy via additive friction stir deposition 通过添加搅拌摩擦沉积实现铸态7075铝合金的强度-塑性协同
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-10-06 DOI: 10.1007/s12289-026-02094-8
Shuaipu Wang, Lei Zhao, Mingjian Wu, Hui Xu, Zihe Xu, Zhilin Wu

As-cast 7075 aluminum alloy suffers from dendritic segregation, coarse second phases, and shrinkage porosity, which limit its direct structural use. In this work, as-cast 7075 feedstock was processed by additive friction stir deposition (AFSD), and the effects of rotation speed on microstructure and mechanical properties were investigated. AFSD markedly reduced casting defects in the as-cast feedstock, with the pore area fraction decreasing from 2.22% to 0.12–0.22% in the deposits. The coarse dendritic structure was transformed into a 3.24–5.16 μm fine-grained microstructure through dynamic-recrystallization-related grain refinement, while interdendritic segregation regions and coarse second phases were fragmented and redistributed as discrete particles. Increasing rotation speed raised the deposition temperature and promoted slight grain coarsening. The deposits showed simultaneous strength and ductility improvements over the as-cast feedstock. The 500 rpm deposit achieved the highest strength, with a yield strength of 320.6 MPa and an ultimate tensile strength of 434.4 MPa, while the highest elongation of 19.0% was obtained at 600 rpm. The improved strength–ductility balance was attributed to grain refinement, pore defect reduction, second-phase fragmentation and redistribution, and local residual deformation. This study demonstrates AFSD as a promising short-process solid-state strategy for as-cast high-strength aluminum alloy feedstocks.

铸态7075铝合金存在枝晶偏析、粗第二相和缩孔,限制了其直接组织应用。采用添加剂搅拌摩擦沉积法(AFSD)对铸态7075进料进行加工,研究了转速对其显微组织和力学性能的影响。AFSD显著降低了铸态原料中的铸造缺陷,其孔隙面积分数从2.22%降至0.12-0.22%。通过动态再结晶细化,粗枝晶组织转变为3.24 ~ 5.16 μm细晶组织,枝晶间偏析区和粗第二相破碎并重新分布为离散颗粒。转速的增加提高了沉积温度,促进了晶粒的轻微粗化。与铸态原料相比,这些沉积层同时表现出强度和延展性的提高。在600 rpm时,合金的屈服强度为320.6 MPa,极限抗拉强度为434.4 MPa,伸长率为19.0%。强度-塑性平衡的改善主要是由于晶粒细化、孔隙缺陷减少、第二相破碎和再分布以及局部残余变形。该研究表明,AFSD是一种很有前途的短工艺固态铸态高强度铝合金原料。
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引用次数: 0
Joining by pin shear caulking: an alternative process route using metallic pins as shear cutting tool 销钉剪切嵌缝连接:使用金属销钉作为剪切切割工具的一种替代工艺路线
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-09-29 DOI: 10.1007/s12289-026-02090-y
L. Elbel, A. Harms, D. Römisch, M. Lechner, M. Merklein

Pin joining represents a promising approach for the mechanical joining of multi-material structures, as it enables the formation of joints without auxiliary joining elements. To improve process efficiency, a modified pin joining process chain is proposed in which the pin itself acts as the cutting element, eliminating the need for pre-drilled joining partners. However, the interactions between the shear-cutting operation and the subsequent caulking process are not yet fully understood. This work experimentally investigates the influence of sheet thickness, relative pin height and cutting clearance on joint formation and mechanical performance in steel-aluminium joints produced by the pin shear-caulking process. A full-factorial design of experiments is employed. Joint performance is evaluated by tensile-shear and cross-tension testing, while metallographic analyses and microhardness measurements are conducted to characterise cut-edge morphology, undercut geometry and local strain hardening. The results demonstrate the feasibility of the proposed process chain and reveal pronounced interactions between the investigated process parameters. Tensile-shear strength is strongly influenced by the interaction between sheet thickness and cutting clearance. A previously reported non-linear effect of cutting clearance is confirmed for a wide range of process conditions and is linked to differences in burnish-zone formation. In contrast, cross-tension strength increases with increasing cutting clearance and is primarily determined by the geometry of the mechanical interlock formed during caulking. Furthermore, increasing sheet thickness and relative pin height generally enhance joint performance by promoting undercut formation and increasing the available load-transfer area. The findings provide a deeper understanding of the mechanisms governing the pin shear-caulking process and support the identification of suitable parameter combinations for future lightweight multi-material structures.

销连接是一种很有前途的多材料结构机械连接方法,因为它可以在没有辅助连接元件的情况下形成连接。为了提高工艺效率,提出了一种改进的销连接工艺链,其中销本身作为切削元件,消除了对预钻连接伙伴的需求。然而,剪切切割操作与随后的填缝过程之间的相互作用尚未完全了解。试验研究了板料厚度、销钉相对高度和切割间隙对销钉剪切嵌缝钢铝接头成形和力学性能的影响。实验采用全因子设计。通过拉伸-剪切和交叉拉伸测试来评估接头性能,同时进行金相分析和显微硬度测量,以表征切割边缘形态、下切几何形状和局部应变硬化。结果证明了所提出的工艺链的可行性,并揭示了所研究的工艺参数之间明显的相互作用。拉伸-剪切强度受板材厚度和切割间隙的相互作用的强烈影响。先前报道的切削间隙的非线性效应在广泛的工艺条件下得到了证实,并与光泽区地层的差异有关。相反,交叉拉伸强度随着切割间隙的增加而增加,主要由填缝过程中形成的机械联锁的几何形状决定。此外,增加板厚和相对销高通常通过促进凹边形成和增加有效载荷传递面积来提高接头性能。这些发现为更深入地理解销剪嵌缝过程的控制机制提供了帮助,并为未来轻质多材料结构确定合适的参数组合提供了支持。
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引用次数: 0
Forming methodology for highly aligned discontinuous fiber composite blanks via epoxy matrix staging 高度对准不连续纤维复合材料坯料环氧基分段成形方法
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-09-29 DOI: 10.1007/s12289-026-02088-6
Matthew Abraham, Thomas A. Cender, Pavel Simacek, Suresh G. Advani

A methodology for rapid manufacturing of complex geometry stretch formed parts from highly aligned discontinuous fiber (ADF) epoxy matrix multiaxial composite blanks is demonstrated in this paper. During typical forming processes, forming and curing occur within the same tool, leading to bottlenecks in processing time. In this new methodology, the epoxy resin is partially cured to increase glass transition temperature above room temperature. Advanced matrix staging allows a blank to be easily removed from a room temperature tool after forming. In a production environment, blanks would be (i) staged in an oven vacuum bag process, (ii) preheated in an IR oven, (iii) rapidly stamp formed into a room temperature tool, (iv) ejected as a near net shape part, and then (v) fully cured/formed in a parallel batch process. To implement this methodology, accurate relationships between viscosity, cure, and glass transition temperature are established and used to manufacture partially cured material for mechanical testing and extensibility characterization. Several key benefits are realized by using partially cured material; namely, the ability to rapidly form and eject a preformed part from tooling and reduced resin bleed during cure and consolidation. The staging process is also shown to retain similar formability and mechanical properties relative to the uncured material form.

介绍了一种由高度对准不连续纤维(ADF)环氧基多轴复合材料毛坯快速制造复杂几何形状拉伸成形件的方法。在典型的成形过程中,成形和固化在同一工具内进行,导致了加工时间的瓶颈。在这种新方法中,环氧树脂部分固化以提高室温以上的玻璃化转变温度。先进的基体分段可以使坯料在成型后很容易地从室温工具中取出。在生产环境中,毛坯将(i)在烘箱真空袋工艺中进行处理,(ii)在红外烘箱中预热,(iii)快速冲压成型为室温工具,(iv)作为接近净形状的部件喷射,然后(v)在平行批处理中完全固化/成型。为了实现这一方法,建立了粘度、固化和玻璃化转变温度之间的精确关系,并用于制造部分固化材料,用于机械测试和可扩展性表征。使用部分固化材料实现了几个关键的好处;也就是说,在固化和固结过程中,快速成型和从模具中弹出预成型零件并减少树脂渗出的能力。与未固化的材料形式相比,分期过程也显示出类似的成形性和机械性能。
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引用次数: 0
Roll pass design for an 18 mm wire rod section using a mill-derived spread-ratio criterion 轧辊孔型设计的18毫米线材部分使用轧机衍生的扩展比准则
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-09-29 DOI: 10.1007/s12289-026-02089-5
Chinta Siva Santosh Dharma Kowshik, Ramesh S, Deepak Kumar, Rajkumar Ohdar

Wire rod is a coiled, round-section steel product hot-rolled from a reheated billet, used as feedstock for wire drawing. Introducing a section beyond an installed mill’s range is constrained by its fixed stand configuration and gear ratios, so that a schedule obtained by simple extension can leave a groove under-filled, a problem addressed sparsely in the literature. This study develops and validates, through a plant trial, a roll pass sequence for 18 mm wire rod meeting dimensional and out-of-roundness requirements without altering the mill’s configuration. The finishing geometry, speed and loads were established analytically for an 18.23 mm hot section. An initial sequence modifying only the last two passes of the block under-filled the round; a lead-bar trial traced the deficit to the pre-finishing oval. A spread ratio, the ratio of imposed reduction to resulting lateral spread per groove, was derived from adjacent validated schedules and adopted as the four-pass design target; the initial two-pass attempt left the side dimension deficient by up to 2.7 mm. The developed four-pass schedule, with reductions of 15.6%, 19.6%, 14.3% and 12.1%, raised the spread ratios to 1.41–3.12, and produced rod measuring 17.95 mm (times ) 17.88 mm at mid-coil, within the ±0.5 mm tolerance, at an ovality of 0.07 mm against a 0.75 mm limit, with loads within the installed drive capacity. The section is now rolled commercially. Expressed as a ratio rather than an absolute spread, it supplies a design target for an unscheduled size; validation here is dimensional.

线材是由再加热的钢坯热轧而成的卷状圆截面钢制品,用作拉丝的原料。引入超出已安装轧机范围的部分受到其固定机架结构和传动比的限制,因此通过简单扩展获得的时间表可能会留下凹槽未填充,这是文献中很少讨论的问题。通过工厂试验,本研究开发并验证了在不改变轧机配置的情况下满足尺寸和圆度要求的18mm线材轧制孔型顺序。分析确定了18.23 mm热断面的精加工几何形状、速度和载荷。一种初始序列,只修改未填充圆的块的最后两遍;一项铅棒试验将缺陷归因于未加工前的椭圆形。扩径比,即从相邻的经过验证的进度表中得出的施加的减小量与每个槽产生的横向扩展量的比值,并将其作为四道设计目标;最初的两次尝试导致侧面尺寸缺陷高达2.7毫米。制定了四关进度表,降低了15.6%%, 19.6%, 14.3% and 12.1%, raised the spread ratios to 1.41–3.12, and produced rod measuring 17.95 mm (times ) 17.88 mm at mid-coil, within the ±0.5 mm tolerance, at an ovality of 0.07 mm against a 0.75 mm limit, with loads within the installed drive capacity. The section is now rolled commercially. Expressed as a ratio rather than an absolute spread, it supplies a design target for an unscheduled size; validation here is dimensional.
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引用次数: 0
Thickness-compensation-driven preform design for hot-press forming of composite hemispherical shells using variable-spacing and variable-angle tow placement 厚度补偿驱动的复合材料半球形壳体热压成形变间距变角度预成形设计
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-09-24 DOI: 10.1007/s12289-026-02085-9
Jiazhong Xu, Shanyu Cao, Meijun Liu, Ze Jin, Yinghao Liu

Non-uniform area deformation during hot-press forming can result in local material accumulation and thickness variation in composite hemispherical shells manufactured from planar tow-placed preforms. This study proposes a thickness-compensation-driven preform design method using variable-spacing and variable-angle tow placement. A geometric inverse mapping relationship is first established between the target hemispherical shell and the planar blank. Based on the local area variation ratio and approximate volume conservation assumption, the formed-thickness requirement is projected back to the planar preform as a spatial material-compensation demand. This compensation demand is subsequently converted into constrained path-spacing, path-density, and local tow-angle distributions. Furthermore, coverage-count statistics are employed to transform discrete tow centerlines into an equivalent initial thickness field for finite element forming analysis.The proposed preform design method is evaluated using an Abaqus/Explicit hot-press forming model and compared with a conventional fixed-angle equal-spacing preform under identical tooling, contact, loading, and mesh conditions. The proposed design reduces the thickness-matching error from 0.024 to 0.019 while satisfying the prescribed minimum curvature-radius constraint of 50 mm. After forming, the thickness standard deviation decreases from 0.231 to 0.171 mm, the coefficient of variation decreases from 14.50% to 10.44%, and the root-mean-square thickness deviation decreases from 0.470 to 0.402 mm. The mean and 95th-percentile von Mises equivalent stresses decrease by 10.7% and 21.1%, respectively, while the mean contact pressure remains at a comparable level. The proposed method establishes a quantitative relationship between planar preform material distribution and formed-thickness control. This framework provides a forward design tool for general double-curvature composite components by linking preform architecture with post-forming thickness uniformity.

在热压成形过程中,非均匀区域变形会导致由平面双置预制件制成的复合半球形壳体的局部材料堆积和厚度变化。提出了一种厚度补偿驱动的变间距变角度拖曳预成形设计方法。首先建立了目标半球形壳体与平面坯料之间的几何逆映射关系。基于局部面积变化率和近似体积守恒假设,将成形厚度需求作为空间材料补偿需求投影回平面预制件。这种补偿需求随后被转换为受限的路径间距、路径密度和局部拖角分布。此外,利用覆盖计数统计将离散的两个中心线转换为等效的初始厚度场,用于有限元成形分析。采用Abaqus/Explicit热压成形模型对所提出的预制件设计方法进行了评估,并在相同的工装、接触、载荷和网格条件下与传统的定角等间距预制件进行了比较。在满足最小曲率半径约束50mm的前提下,将厚度匹配误差从0.024减小到0.019。成形后,厚度标准差从0.231 mm减小到0.171 mm,变异系数从14.50%减小到10.44%,均方根厚度偏差从0.470 mm减小到0.402 mm。平均和95百分位von Mises等效应力分别下降10.7%和21.1%,而平均接触压力保持在可比水平。该方法建立了平面预制件材料分布与成形厚度控制之间的定量关系。该框架通过将预制体结构与成型后厚度均匀性联系起来,为一般双曲率复合材料构件的正向设计提供了工具。
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引用次数: 0
Effect of amplitude on microstructure and properties of hot oscillating pressure sintering AlCoCrNiFe high-entropy alloys 振幅对热振荡压力烧结AlCoCrNiFe高熵合金组织和性能的影响
IF 2.6 3区 材料科学 Q2 ENGINEERING, MANUFACTURING Pub Date : 2026-09-21 DOI: 10.1007/s12289-026-01986-z
Ka Gao, Yuan Rao, Teng Fang, Yuhang Han, Yufan Tang, Wei Chen, Ziheng Gao, Furong Xie, Bin Chen, Chuan Li

This work employs the hot oscillatory pressure (HOP) sintering technique for the first time to prepare AlCoCrNiFe high-entropy alloy at varying amplitudes, systematically investigating the influence of amplitude on their microstructure and properties. As the amplitude increased, the grain boundaries of HOP sintered alloy were disappeared, and significant improvements in density and microstructural uniformity were observed. Specifically, when the amplitude increased from ± 1 to ± 10 MPa, the density of the HOP sintered alloy was rose from 93.65% to 99.11%, achieving near-complete densification. The increased amplitude also effectively enhanced their hardness and corrosion resistance. At an amplitude of ± 10 MPa, the Vickers hardness of the HOP sintered AlCoCrNiFe high-entropy alloy was reached a maximum of 481.52 HV1, which was significantly higher than that of the hot-press sintered samples. Moreover, its corrosion current density was minimized at 9.1 µA/cm², indicating the strongest corrosion resistance. The research results demonstrate that the increasing the HOP amplitude can produce high-entropy alloys with high density, well hardness, and excellent corrosion resistance in lower temperature.

本文首次采用热振荡压力(HOP)烧结技术制备了变振幅下的AlCoCrNiFe高熵合金,系统地研究了振幅对其组织和性能的影响。随着振幅的增大,HOP烧结合金的晶界逐渐消失,密度和组织均匀性显著提高。当振幅从±1 MPa增加到±10 MPa时,HOP烧结合金的密度从93.65%提高到99.11%,接近完全致密化。振幅的增加也有效地提高了材料的硬度和耐蚀性。在±10 MPa振幅下,HOP烧结AlCoCrNiFe高熵合金的维氏硬度达到最大值481.52 HV1,显著高于热压烧结试样。腐蚀电流密度最小,为9.1µA/cm²,耐蚀性最强。研究结果表明,增大HOP振幅可以制备出密度高、硬度好、耐低温腐蚀性能优异的高熵合金。
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International Journal of Material Forming
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