This work employs the hot oscillatory pressure (HOP) sintering technique for the first time to prepare AlCoCrNiFe high-entropy alloy at varying amplitudes, systematically investigating the influence of amplitude on their microstructure and properties. As the amplitude increased, the grain boundaries of HOP sintered alloy were disappeared, and significant improvements in density and microstructural uniformity were observed. Specifically, when the amplitude increased from ± 1 to ± 10 MPa, the density of the HOP sintered alloy was rose from 93.65% to 99.11%, achieving near-complete densification. The increased amplitude also effectively enhanced their hardness and corrosion resistance. At an amplitude of ± 10 MPa, the Vickers hardness of the HOP sintered AlCoCrNiFe high-entropy alloy was reached a maximum of 481.52 HV1, which was significantly higher than that of the hot-press sintered samples. Moreover, its corrosion current density was minimized at 9.1 µA/cm², indicating the strongest corrosion resistance. The research results demonstrate that the increasing the HOP amplitude can produce high-entropy alloys with high density, well hardness, and excellent corrosion resistance in lower temperature.


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