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Palbociclib Letrozole Loaded Liquid Crystaline Nanoparticles for Treatment of Breast Cancer : Design, Optimization, In-Vitro Evaluation and In-Vivo Characterization 帕博西尼来曲唑负载液晶纳米颗粒治疗乳腺癌:设计,优化,体外评价和体内表征
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-12 DOI: 10.1007/s12247-026-11118-4
Umesh B. Kolap, Himmat Singh Chawra, Sunil T. Galatage

Current research work aimed to develop and characterise of liquid crystalline nanoparticles (LCNPs) physically blended dual-LCNP formulation with palbociclib (PCB) and letrozole (LTZ) to improve therapeutic performance in treatment of breast cancer. Drug-loaded LCNPs were prepared using glyceryl monooleate (GMO) as the lipid phase and Poloxamer-407 as the stabilizer via a high-energy emulsification followed by probe sonication. A 3² full factorial design was applied to systematically optimize critical formulation variables affecting particle size and entrapment efficiency. The optimized LCNs of dispersions were combined to obtain the final formulation (PLNs-9) and characterized for morphology (TEM), thermal behaviour (DSC), crystallinity (XRD), and drug–excipient compatibility (FTIR). The PLNs-9 exhibited nanoscale particle size (144.2 ± 5.3 nm) with high entrapment efficiencies (PCB 95.54 ± 3.57%, LTZ 84.35 ± 2.86%). Solid-state analyses confirmed molecular dispersion of drugs within the lipid matrix. In vitro release studies demonstrated sustained drug release under physiological conditions. Cytotoxicity studies in MCF-7 breast cancer cells revealed significantly enhanced antiproliferative activity of PLNs-9 (IC₅₀ = 10.56 ± 1.34 µg; p < 0.001) compared with individual drugs and their physical combination, accompanied by increased apoptotic cell populations and pronounced G2/M phase arrest. Pharmacokinetic evaluation demonstrated prolonged systemic circulation and approximately 2-fold enhancement in relative bioavailability compared to both PCB and LTZ. These findings suggest that the developed PLNs-9 containing PCB and LTZ combination represents a promising synergistic nanotherapeutic platform for breast cancer management.

目前的研究工作旨在开发和表征液晶纳米颗粒(LCNPs)与帕博西尼(PCB)和来曲唑(LTZ)物理混合的双lcnp配方,以提高治疗乳腺癌的疗效。以单油酸甘油酯(GMO)为脂相,poloxmer -407为稳定剂,经高能乳化后探针超声制备了载药LCNPs。采用3²全因子设计对影响粒径和捕集效率的关键配方变量进行了系统优化。将优化后的分散体LCNs组合得到最终配方(PLNs-9),并对其形貌(TEM)、热行为(DSC)、结晶度(XRD)和药物赋形剂相容性(FTIR)进行表征。PLNs-9具有纳米级粒径(144.2±5.3 nm)和较高的包封效率(PCB为95.54±3.57%,LTZ为84.35±2.86%)。固态分析证实了药物在脂质基质中的分子分散。体外释放研究表明药物在生理条件下持续释放。MCF-7乳腺癌细胞的细胞毒性研究显示,与单个药物及其物理组合相比,PLNs-9 (IC₅₀= 10.56±1.34µg; p < 0.001)的抗增殖活性显着增强,伴有凋亡细胞群增加和明显的G2/M期阻滞。药代动力学评价表明,与多氯联苯和LTZ相比,其体循环延长,相对生物利用度提高约2倍。这些发现表明,开发的含有PCB和LTZ组合的PLNs-9代表了一个有希望的乳腺癌管理协同纳米治疗平台。
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引用次数: 0
In Silico Identification and Mechanistic Characterization of Cyanobacterial Metabolites as Potential CD38 Inhibitors for Multiple Myeloma 蓝藻代谢物作为多发性骨髓瘤潜在CD38抑制剂的硅鉴定和机制表征
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-12 DOI: 10.1007/s12247-026-11102-y
Xiaoyi Dun, Shuang Chen, Qinfen Wu

Multiple myeloma (MM) is an incurable plasma cell malignancy characterized by dysregulation of CD38, a multifunctional ectoenzyme and receptor critical for tumor progression and immune modulation. While monoclonal antibodies targeting CD38 have improved clinical outcomes, small-molecule inhibitors remain scarce, limiting alternative therapeutic strategies. In this study, we employed a comprehensive in silico approach to identify drug-like, non-toxic marine Cyanobacterial metabolites as promising potential CD38 inhibitors. A total of 1085 MM-associated genes were intersected with 357 CD38-interacting genes to identify 207 MM-associated targets, which were enriched in immune-regulatory pathways. The CD38 binding pocket was characterized, and molecular docking screened Cyanobacterial metabolites for binding affinity and drug-likeness, identifying top candidates compliant with Lipinski, Ghose, Veber, Egan, and Muegge rules. Based on binding affinity, the selected drug-like, non-toxic metabolites (CyanoMetDB_1359, CyanoMetDB_2811, and CyanoMetDB_2812) exhibited favorable interactions with key residues, including TRP125, LEU145, TRP176, and THR221, overlapping with co-crystallized ligand interactions. Molecular dynamics simulations over 200 ns revealed stable protein-ligand complexes, with consistent RMSD, RMSF, Rg, SASA, distance, and hydrogen-bond profiles. Extensive principal component analysis and free energy landscapes confirmed conformational stability and minimal fluctuation. MM-PBSA calculations indicated favorable binding free energies, with residue-based decomposition suggesting critical stabilizing interactions. Collectively, this study identifies rare, marine-derived small-molecule candidates capable of effectively targeting CD38, bridging marine natural product chemistry with MM therapeutics. These findings provide a foundation for future experimental validation and development of small-molecule CD38 inhibitors derived from natural sources, with potential anti-myeloma activity.

多发性骨髓瘤(MM)是一种无法治愈的浆细胞恶性肿瘤,其特征是CD38失调,CD38是一种多功能外酶和受体,对肿瘤进展和免疫调节至关重要。虽然靶向CD38的单克隆抗体改善了临床结果,但小分子抑制剂仍然稀缺,限制了其他治疗策略。在这项研究中,我们采用了一种综合的计算机方法来鉴定类似药物的、无毒的海洋蓝藻代谢物作为潜在的CD38抑制剂。共有1085个mm相关基因与357个cd38相互作用基因相交,鉴定出207个mm相关靶点,这些靶点在免疫调节途径中富集。对CD38结合袋进行了表征,并对蓝藻代谢产物进行了分子对接筛选,以确定其结合亲和力和药物相似性,并确定了符合Lipinski, Ghose, Veber, Egan和Muegge规则的最佳候选物。基于结合亲和力,所选择的药物样、无毒代谢物(CyanoMetDB_1359、CyanoMetDB_2811和CyanoMetDB_2812)与关键残基(包括TRP125、LEU145、TRP176和THR221)表现出良好的相互作用,并与共结晶配体相互作用重叠。在200 ns的分子动力学模拟中,发现了稳定的蛋白质配体复合物,具有一致的RMSD、RMSF、Rg、SASA、距离和氢键谱。广泛的主成分分析和自由能景观证实了构象的稳定性和最小的波动。MM-PBSA计算显示了良好的结合自由能,残基分解表明了关键的稳定相互作用。总的来说,本研究确定了罕见的,能够有效靶向CD38的海洋衍生小分子候选药物,将海洋天然产物化学与MM治疗方法连接起来。这些发现为未来实验验证和开发天然来源的具有潜在抗骨髓瘤活性的小分子CD38抑制剂提供了基础。
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引用次数: 0
Co-delivery of Quercetin and Resveratrol via Polymeric Nanoparticles for Enhanced Therapeutic Efficacy Against Colorectal Cancer 槲皮素和白藜芦醇通过聚合物纳米颗粒共同递送增强对结直肠癌的治疗效果
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-10 DOI: 10.1007/s12247-026-11100-0
Kumar Janakiraman, Vaidevi Sethuraman, Geethanjali Sampath, Venkateshwaran Krishnaswami

Background

Colorectal cancer (CRC) remains a major global health burden, emphasizing the need for targeted therapies with improved efficacy and fewer adverse effects. Quercetin and resveratrol possess substantial anticancer activity, but their therapeutic application is limited by poor bioavailability, instability, and rapid degradation.

Methods

Quercetin- and resveratrol-co-loaded polymeric nanoparticles (QRNPs) were formulated using poly(lactic-co-glycolic acid) (PLGA) and D-α-tocopheryl polyethylene glycol succinate (TPGS). The optimized formulation was evaluated for particle size, zeta potential, encapsulation efficiency, morphology, drug–polymer compatibility, pH-dependent drug release, gastrointestinal stability, cellular uptake, cytotoxicity, and apoptosis in Caco-2 colorectal cancer cells.

Results

Optimized QRNPs showed a particle size of 174–177 nm, zeta potential of approximately −22 to −24 mV, and encapsulation efficiency above 80%. FTIR analysis confirmed drug–polymer compatibility, while HR-TEM revealed uniform spherical morphology. Drug-release studies demonstrated minimal release at pH 7.4 and increased release at pH 5.5, indicating preferential release under acidic tumor-like conditions. QRNPs also remained stable in simulated gastrointestinal fluids, demonstrating formulation robustness. Compared with free quercetin and resveratrol, QRNPs produced greater cytotoxicity, with CC50 values of 48.84 μg/mL at 24 h and 32.75 μg/mL at 48 h. Fluorescence imaging demonstrated enhanced cellular uptake, and Annexin V-FITC analysis confirmed increased apoptosis in treated cells.

Conclusion

PLGA–TPGS-based quercetin–resveratrol nanoparticles improved drug stability, cellular uptake, pH-responsive release, gastrointestinal robustness, and in-vitro anticancer activity. These findings support their potential as a promising nanocarrier system for improving colorectal cancer therapy through efficient co delivery of quercetin and resveratrol, while potentially reducing limitations of free drugs.

Graphical Abstract

结直肠癌(CRC)仍然是一个主要的全球健康负担,强调需要靶向治疗,以提高疗效和减少不良反应。槲皮素和白藜芦醇具有很强的抗癌活性,但由于生物利用度差、不稳定和降解快,限制了它们的治疗应用。方法采用聚乳酸-羟基乙酸(PLGA)和D-α-生育酚聚乙二醇琥珀酸酯(TPGS)制备槲皮素和白藜芦醇共载聚合物纳米粒子(QRNPs)。在Caco-2结直肠癌细胞中,对优化后的制剂进行了粒径、zeta电位、包封效率、形态、药物-聚合物相容性、ph依赖性药物释放、胃肠道稳定性、细胞摄取、细胞毒性和凋亡的评估。结果优化后的QRNPs的粒径为174 ~ 177 nm, zeta电位约为−22 ~−24 mV,包封率在80%以上。FTIR分析证实了药物-聚合物相容性,而HR-TEM显示了均匀的球形形貌。药物释放研究表明,pH为7.4时释放最小,pH为5.5时释放增加,表明在酸性肿瘤样条件下优先释放。QRNPs在模拟胃肠道液体中也保持稳定,证明了配方的稳健性。与游离槲皮素和白藜芦醇相比,QRNPs具有更强的细胞毒性,24 h和48 h的CC50值分别为48.84 μg/mL和32.75 μg/mL。荧光成像显示细胞摄取增强,Annexin V-FITC分析证实处理后细胞凋亡增加。结论基于plga - tpgs的槲皮素-白藜芦醇纳米颗粒提高了药物稳定性、细胞摄取、ph响应释放、胃肠稳受性和体外抗癌活性。这些发现支持了它们作为一种有前途的纳米载体系统的潜力,通过槲皮素和白藜芦醇的有效联合递送,改善结直肠癌的治疗,同时有可能减少免费药物的局限性。图形抽象
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引用次数: 0
Design, Characterization, and Evaluation of a Thermogelling Intranasal Delivery System of Rasagiline Mesylate for Brain Targeting 甲磺酸雷沙吉兰脑靶向热凝胶鼻内给药系统的设计、表征和评价
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-10 DOI: 10.1007/s12247-026-11104-w
Dumpa Rushi Kumar Reddy, Suryaprakash Reddy Chappidi

Background

Parkinson’s Disease is the second most common neurodegenerative disorder worldwide. Although levodopa and monoamine oxidase-B (MAO-B) inhibitors remain the cornerstone of symptomatic management, oral administration is often limited by poor brain targeting and restricted penetration across the blood–brain barrier. The present study aimed to develop and optimize a thermoresponsive nasal in situ gel of Rasagiline Mesylate (RM) to facilitate direct nose-to-brain delivery.

Materials and Methods

A Central Composite Design (CCD) was employed to optimize the formulation. Poloxamer 407 (A: 15–30%, including axial points of 11.89 and 33.11%) and dodecyl maltoside (B: 1.0–2.0%, including axial points of 0.79 and 2.21%) were selected as independent variables, while gelation time, mucoadhesive strength, and permeation coefficient were considered response variables. The developed formulations were characterized for gelation time, mucoadhesive strength, drug content, pH, gelation temperature, viscosity, in vitro permeation, droplet size distribution, and plume geometry.

Results

The optimized formulation (RM1; 22.5% Poloxamer 407 and 1.5% dodecyl maltoside) demonstrated rapid thermogelation at physiological temperature (30.21 s), favourable mucoadhesive strength (~ 1615.8 dyne/cm²), and an enhanced permeation coefficient (0.0029 cm/s). In contrast, formulations containing higher polymer concentrations (RM10; 30% Poloxamer 407 and 2% dodecyl maltoside) exhibited prolonged gelation and reduced permeation performance. All formulations maintained a pH of approximately 7.3, indicating suitability for nasal administration. The optimized gel also exhibited acceptable spray characteristics, viscosity, and drug content uniformity.

Conclusion

The optimized thermosensitive nasal in situ gel of rasagiline mesylate demonstrated desirable physicochemical properties, mucoadhesion, and permeation behaviour, supporting its potential as a non-invasive nose-to-brain delivery platform. This approach may enhance central nervous system targeting of MAO-B inhibitors and represents a promising strategy for improving therapeutic outcomes in Parkinson’s disease.

帕金森氏病是世界上第二常见的神经退行性疾病。尽管左旋多巴和单胺氧化酶- b (MAO-B)抑制剂仍然是症状治疗的基础,但口服给药往往受到脑靶向性差和穿过血脑屏障的渗透受限的限制。本研究旨在开发和优化甲磺酸雷沙吉兰(RM)热反应性鼻腔原位凝胶,以促进直接鼻至脑给药。材料与方法采用中心复合设计(CCD)优化配方。选取Poloxamer 407 (A: 15-30%,轴向点分别为11.89和33.11%)和十二烷基麦芽糖苷(B: 1.0-2.0%,轴向点分别为0.79和2.21%)作为自变量,以胶凝时间、粘接强度和渗透系数为响应变量。通过凝胶时间、粘接强度、药物含量、pH值、凝胶温度、粘度、体外渗透、液滴大小分布和羽流几何形状对所开发的配方进行了表征。结果优化后的配方(RM1; 22.5% poloxam407和1.5%十二烷基麦糖苷)在生理温度下热凝胶反应快(30.21 s),粘接强度高(~ 1615.8 dyne/cm²),渗透系数提高(0.0029 cm/s)。相比之下,含有较高聚合物浓度(RM10; 30% poloxam407和2%十二烷基麦芽糖)的配方表现出长时间的凝胶化和降低的渗透性能。所有制剂的pH值保持在7.3左右,表明适合鼻腔给药。优化后的凝胶还具有可接受的喷雾特性、粘度和药物含量均匀性。结论经优化的甲磺酸雷沙吉兰热敏鼻腔原位凝胶具有良好的理化性能、黏附性和渗透性,具有作为无创鼻脑给药平台的潜力。这种方法可以增强中枢神经系统对MAO-B抑制剂的靶向作用,并代表了一种改善帕金森病治疗结果的有希望的策略。
{"title":"Design, Characterization, and Evaluation of a Thermogelling Intranasal Delivery System of Rasagiline Mesylate for Brain Targeting","authors":"Dumpa Rushi Kumar Reddy,&nbsp;Suryaprakash Reddy Chappidi","doi":"10.1007/s12247-026-11104-w","DOIUrl":"10.1007/s12247-026-11104-w","url":null,"abstract":"<div><h3>Background</h3><p>Parkinson’s Disease is the second most common neurodegenerative disorder worldwide. Although levodopa and monoamine oxidase-B (MAO-B) inhibitors remain the cornerstone of symptomatic management, oral administration is often limited by poor brain targeting and restricted penetration across the blood–brain barrier. The present study aimed to develop and optimize a thermoresponsive nasal in situ gel of Rasagiline Mesylate (RM) to facilitate direct nose-to-brain delivery.</p><h3>Materials and Methods</h3><p>A Central Composite Design (CCD) was employed to optimize the formulation. Poloxamer 407 (A: 15–30%, including axial points of 11.89 and 33.11%) and dodecyl maltoside (B: 1.0–2.0%, including axial points of 0.79 and 2.21%) were selected as independent variables, while gelation time, mucoadhesive strength, and permeation coefficient were considered response variables. The developed formulations were characterized for gelation time, mucoadhesive strength, drug content, pH, gelation temperature, viscosity, in vitro permeation, droplet size distribution, and plume geometry.</p><h3>Results</h3><p>The optimized formulation (RM1; 22.5% Poloxamer 407 and 1.5% dodecyl maltoside) demonstrated rapid thermogelation at physiological temperature (30.21 s), favourable mucoadhesive strength (~ 1615.8 dyne/cm²), and an enhanced permeation coefficient (0.0029 cm/s). In contrast, formulations containing higher polymer concentrations (RM10; 30% Poloxamer 407 and 2% dodecyl maltoside) exhibited prolonged gelation and reduced permeation performance. All formulations maintained a pH of approximately 7.3, indicating suitability for nasal administration. The optimized gel also exhibited acceptable spray characteristics, viscosity, and drug content uniformity.</p><h3>Conclusion</h3><p>The optimized thermosensitive nasal in situ gel of rasagiline mesylate demonstrated desirable physicochemical properties, mucoadhesion, and permeation behaviour, supporting its potential as a non-invasive nose-to-brain delivery platform. This approach may enhance central nervous system targeting of MAO-B inhibitors and represents a promising strategy for improving therapeutic outcomes in Parkinson’s disease.</p></div>","PeriodicalId":656,"journal":{"name":"Journal of Pharmaceutical Innovation","volume":"22 1","pages":""},"PeriodicalIF":2.6,"publicationDate":"2026-10-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"149188897","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Liraglutide as a Novel Strategy for Improving Metabolic and Hormonal Profiles in Obese Women with Polycystic Ovary Syndrome 利拉鲁肽作为改善肥胖多囊卵巢综合征妇女代谢和激素谱的新策略
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-10 DOI: 10.1007/s12247-026-10995-z
Sara Medhat Georgy, Nada Farag Elnaidany, Nora A Abdelmoneum, Sara Abdallah Mohamed Salem, Heba F. Salem, Rania M. Sarhan

Purpose

This study aimed to investigate the effect of liraglutide and metformin as monotherapies on the hormonal, metabolic and clinical parameters of Poly Cystic Ovary Syndrome (PCOS). Participants were assigned to receive either Liraglutide (gradually titrated up to 3.0 mg/day as tolerated), Metformin (1000 mg/day), or standard lifestyle modification as a control group for 6 months.

Methods

A randomized, parallel, clinical trial was conducted on 150 patients (50 per group) who completed the study, out of 183 initially randomized patients diagnosed with PCOS.

Results

Out of 183 randomized patients, 150 completed the 24-week protocol (n = 50 per group). Most baseline characteristics were comparable across groups. Following 24 weeks of treatment, baseline-adjusted linear regression demonstrated that liraglutide induced significantly greater weight reduction compared to control (adjusted mean difference: -10.13 kg, FDR-adjusted p < 0.001). Furthermore, liraglutide yielded substantial improvements in insulin resistance, as evidenced by a significantly lower HOMA-IR compared to control (adjusted mean difference: -0.58, FDR-adjusted p < 0.001). Menstrual cycle regularity markedly improved in the liraglutide group (76.0%) compared to metformin (50.0%) and control (32.0%) (p < 0.001). Clinical pregnancy rates were 29.0% Control, 65.7% Liraglutide, 52.9% Metformin; overall between-group difference remained significant after FDR correction (χ²=9.026, FDR-adjusted p=0.044). Nausea, heartburn, and constipation were more frequent with liraglutide than metformin.

Conclusion

Liraglutide is significantly more effective than metformin in improving body weight, glycemic control, and menstrual frequency in women with PCOS and metabolic dysfunction. These findings support liraglutide as a primary therapeutic approach, particularly in obesity-associated PCOS. It was registered at ClinicalTrials.gov under the identifier NCT05965908, registered on July 20, 2023.

目的探讨利拉鲁肽联合二甲双胍单药治疗对多囊卵巢综合征(PCOS)患者激素、代谢及临床指标的影响。参与者被分配接受利拉鲁肽(逐渐滴定至耐受的3.0 mg/天)、二甲双胍(1000 mg/天)或标准生活方式改变作为对照组,为期6个月。方法在183例最初被随机诊断为多囊卵巢综合征的患者中,对150例完成研究的患者(每组50例)进行了一项随机、平行、临床试验。结果183例随机患者中,150例完成了24周的治疗方案(每组50例)。大多数基线特征在各组间具有可比性。治疗24周后,基线校正线性回归显示,利拉鲁肽诱导的体重减轻明显大于对照组(校正平均差:-10.13 kg,经fdr校正p <; 0.001)。此外,利拉鲁肽显著改善了胰岛素抵抗,与对照组相比,HOMA-IR显著降低(校正平均差:-0.58,fdr校正p <; 0.001)。与二甲双胍组(50.0%)和对照组(32.0%)相比,利拉鲁肽组(76.0%)的月经周期规律明显改善(p < 0.001)。临床妊娠率:对照组29.0%,利拉鲁肽65.7%,二甲双胍52.9%;经FDR校正后,总体组间差异仍有统计学意义(χ²=9.026,经FDR校正的p=0.044)。利拉鲁肽比二甲双胍更容易引起恶心、胃灼热和便秘。结论利拉鲁肽在改善PCOS合并代谢功能障碍患者体重、血糖控制和月经频率方面明显优于二甲双胍。这些发现支持利拉鲁肽作为主要的治疗方法,特别是在肥胖相关的多囊卵巢综合征。它已于2023年7月20日在ClinicalTrials.gov注册,注册标识符为NCT05965908。
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引用次数: 0
Hydrophilic DNA Conjugation in HPMC Films: A Strategy for Poorly Soluble Drugs HPMC膜中的亲水性DNA偶联:一种用于难溶性药物的策略
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-10 DOI: 10.1007/s12247-026-11121-9
Debashis Purohit, Amit Kumar Nayak, Mahendra Kumar Sahu, Aakanksha Sinha, Prince Kumar Jha

The study examined the effect of DNA conjugation on the solubility of a drug in an HPMC polymeric film. The study found that incorporating DNA extract in the film improved drug solubility. The formulation NHE5, with 20% bioplasticizer, showed better drug release compared to other formulations. FTIR and DSC and XRD analyses were carried out. This study indicates that a promising development in drug delivery technology is DNA conjugation to HPMC polymeric films. DNA-HPMC conjugates can enhance DNA-functionalized polymers, promizing improved drug delivery systems and maximizing therapeutic efficacy in pharmaceutical formulations.

Graphical Abstract

本研究考察了DNA偶联对药物在HPMC聚合物膜中的溶解度的影响。研究发现,在薄膜中加入DNA提取物可以提高药物的溶解度。与其他制剂相比,添加20%生物增塑剂的制剂NHE5具有较好的释药效果。进行了FTIR、DSC和XRD分析。这项研究表明,DNA与HPMC聚合物膜的结合是药物传递技术的一个有前途的发展方向。DNA-HPMC缀合物可以增强dna功能化聚合物,有望改善药物传递系统并最大限度地提高药物制剂的治疗效果。图形抽象
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引用次数: 0
Thermo-Responsive Hydrogels Loaded with Holothuria atra Silver–Chitosan Nanocomposites for Burn Wound Healing: A Network Pharmacology-Guided Study 负载银壳聚糖纳米复合材料的热响应水凝胶用于烧伤创面愈合:网络药理学指导的研究
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-10 DOI: 10.1007/s12247-026-11107-7
Basant A. Abou-Taleb, Zeinab M. Awwad, Dina S. Ghallab

Purpose

Wound healing remains a major clinical challenge, particularly in conditions characterized by excessive inflammation and impaired angiogenesis. To address this, the present study was designed to develop and evaluate biocompatible, eco-friendly nano-gels that modulate inflammation and enhance vascularization to accelerate tissue repair.

Methods

Three Holothuria atra extract-loaded nano-systems, chitosan nanoparticles (CS NPs), silver nanoparticles (Ag NPs), and chitosan-coated silver nanoparticles (CS-Ag NPs), were green-synthesized, incorporated into a thermo-responsive poloxamer 407/sodium hyaluronate in situ gel, and evaluated for wound-healing efficacy. Network pharmacology was applied to systematically decipher the multi-target mechanisms of H. atra bioactives and guide biomarker selection.

Results

Network pharmacology identified MAPK1, IL6, AKT1, TNF, and VEGFA as central hub genes prominently enriched in the MAPK, PI3K-Akt, TNF-α, and VEGF signaling pathways, highlighting the multi-target mechanism of H. atra bioactives. Physicochemical characterization demonstrated an optimal gelling temperature (32–34 °C), rapid gelation time (50–55 s), skin-compatible pH (5.8–6.2), and pseudoplastic rheological behavior. In vitro release studies confirmed sustained drug release from the nano-gel formulations compared to the unformulated extract solution, with the CS-Ag NP gel exhibiting superior controlled-release performance. In a Sprague-Dawley rat burn model, the nano-gel formulations significantly accelerated wound closure; the H. atra-CS-Ag NP gel achieved a leading wound contraction of 71.72 ± 2.5% by day 12, comparable to the commercial standard HYALO® 4 Control (70.18 ± 2.9%). Biochemical analysis revealed significant downregulation of pro-inflammatory cytokines (TNF-α and IL-6) alongside elevated expression of angiogenic and repair markers (VEGFA, AKT1, and MAPK1). Furthermore, in vitro–in vivo correlation (IVIVC) analysis demonstrated strong linear relationships between in vitro dissolution efficiency and network pharmacology-guided biomarkers (r² ≥ 0.922, p ≤ 0.05), confirming a novel systems-level therapeutic approach.

Conclusion

Overall, integrating marine-derived bioactives, silver-chitosan nanotechnology, and thermo-responsive hydrogels offers a promising synergistic platform for advanced wound therapy.

伤口愈合仍然是一个主要的临床挑战,特别是在过度炎症和血管生成受损的情况下。为了解决这个问题,本研究旨在开发和评估生物相容性,生态友好的纳米凝胶,以调节炎症和增强血管化,加速组织修复。方法绿色合成壳聚糖纳米粒子(CS- NPs)、银纳米粒子(Ag - NPs)和壳聚糖包被银纳米粒子(CS-Ag - NPs),并将其加入到热响应性波洛沙姆407/透明质酸钠原位凝胶中,评价其创面愈合效果。应用网络药理学技术,系统地破译了H. atra生物活性的多靶点机制,并指导了生物标志物的选择。结果网络药理学鉴定MAPK1、IL6、AKT1、TNF和VEGFA为中心枢纽基因,在MAPK、PI3K-Akt、TNF-α和VEGF信号通路中显著富集,突出了H. atra生物活性的多靶点机制。理化特性证明了最佳胶凝温度(32-34℃)、快速胶凝时间(50-55 s)、皮肤相容pH值(5.8-6.2)和假塑性流变行为。体外释放研究证实,与未配制的提取液相比,纳米凝胶制剂具有持续的药物释放,其中CS-Ag NP凝胶具有更好的控释性能。在Sprague-Dawley大鼠烧伤模型中,纳米凝胶制剂显著加速伤口愈合;H. atra-CS-Ag NP凝胶在第12天的伤口收缩率为71.72±2.5%,与商业标准HYALO®4 Control(70.18±2.9%)相当。生化分析显示,促炎细胞因子(TNF-α和IL-6)显著下调,血管生成和修复标志物(VEGFA、AKT1和MAPK1)表达升高。此外,体外相关(IVIVC)分析显示,体外溶出效率与网络药理学引导的生物标志物之间存在很强的线性关系(r²≥0.922,p≤0.05),证实了一种新的系统级治疗方法。综上所述,将海洋生物活性物质、银壳聚糖纳米技术和热反应性水凝胶相结合,为先进创面治疗提供了一个有前景的协同平台。
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引用次数: 0
Development and Validation of a UHPLC–MS/MS Method for Trace-Level Determination of N-Nitroso Chlordiazepoxide in Chlordiazepoxide Hydrochloride Capsule Dosage Form 超高效液相色谱-质谱联用法测定盐酸氯二氮环氧酯胶囊剂型中n -亚硝基氯二氮环氧酯的含量及验证
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-09 DOI: 10.1007/s12247-026-11113-9
Rajamani Dhanasekar, Vadivel Velmurugan, Sankham Devendran Rajendran

Background

Nitrosamine impurities are a significant pharmaceutical quality concern because of their potential mutagenic and carcinogenic effects. Sensitive and reliable analytical methods are required for their determination in pharmaceutical dosage forms.

Objective

This study aimed to develop and validate a sensitive and selective ultra-high-performance liquid chromatography–tandem mass spectrometry (UHPLC–MS/MS) method for the trace-level determination of N-nitrosochlordiazepoxide (NNC) in chlordiazepoxide hydrochloride capsule dosage forms.

Methods

Chromatographic separation was achieved using an X-Select HSS C18 XP column (150 × 4.6 mm, 3.5 μm) with gradient elution. Detection was performed using a triple quadrupole mass spectrometer in positive electrospray ionization mode with multiple reaction monitoring (MRM) at m/z 329.10 → 282.10. The method was validated for specificity, linearity, sensitivity, precision, accuracy, solution stability, and filter compatibility in accordance with ICH Q2(R2) recommendations.

Results

The method demonstrated no interference from blank, placebo, or formulation matrix components. Linearity was established over the concentration range of 0.1732–0.6929 ppm, with a coefficient of determination (R²) of 1.000. The limit of detection (LOD) and limit of quantification (LOQ) were 0.052 and 0.1732 ppm, respectively. Method precision and intermediate precision showed %RSD values of 14.1% and 1.2%, respectively, with a cumulative %RSD of 10.4%. Accuracy studies demonstrated mean recoveries of 85–86% across the LOQ, 100%, and 200% concentration levels, with %RSD values of 0.7–1.1%. Standard and sample solutions remained stable for 13 h and 2 h, respectively, under refrigerated conditions. Analysis of commercial 10 mg and 25 mg capsule samples showed that NNC was not detected in any of the tested batches.

Conclusion

The developed UHPLC–MS/MS method demonstrated sensitivity and specificity for trace-level NNC determination in chlordiazepoxide hydrochloride capsule dosage forms. Although the method showed good intermediate precision and consistent recovery, the observed method-precision variability and potential under-recovery should be considered when interpreting quantitative results. The method was successfully applied to the tested commercial capsule batches, in which NNC was not detected under the analytical conditions employed.

Graphical Abstract

亚硝胺类杂质是一个重要的药品质量问题,因为它们具有潜在的致突变和致癌作用。需要灵敏、可靠的分析方法来测定药物剂型中它们的含量。目的建立灵敏、选择性的超高效液相色谱-串联质谱(UHPLC-MS /MS)法测定盐酸氯二氮吡酯胶囊剂型中n -亚硝基氯二氮吡酯(NNC)的含量。方法采用X-Select HSS C18 XP色谱柱(150 × 4.6 mm, 3.5 μm)梯度洗脱进行色谱分离。在m/z 329.10→282.10的正电喷雾电离模式下,采用多重反应监测(MRM)三重四极杆质谱仪进行检测。根据ICH Q2(R2)建议,验证了该方法的特异性、线性度、灵敏度、精密度、准确度、溶液稳定性和过滤器兼容性。结果该方法不受空白、安慰剂或制剂基质成分的干扰。在0.1732 ~ 0.6929 ppm的浓度范围内建立线性关系,决定系数(R²)为1.000。检出限为0.052 ppm,定量限为0.1732 ppm。方法精密度和中间精密度%RSD分别为14.1%和1.2%,累计%RSD为10.4%。准确度研究表明,在LOQ、100%和200%浓度水平上,平均回收率为85-86%,%RSD值为0.7-1.1%。标准溶液和样品溶液在冷藏条件下分别保持稳定13h和2h。对商业10毫克和25毫克胶囊样品的分析表明,在任何测试批次中均未检测到NNC。结论建立的超高效液相色谱-质谱联用方法对盐酸氯二氮环氧酯胶囊剂型中微量非分子控制含量的测定具有良好的敏感性和特异性。虽然该方法具有良好的中间精密度和一致的回收率,但在解释定量结果时应考虑观察到的方法精密度变异性和潜在的欠回收率。该方法成功地应用于所测试的商业胶囊批次,在所采用的分析条件下未检测到NNC。图形抽象
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引用次数: 0
A Hybrid Nano-ODT Platform: Merging Freeze-Drying and Nanosuspension Technologies to Overcome Loratadine’s Dissolution Limitation 混合纳米odt平台:结合冷冻干燥和纳米悬浮液技术克服氯雷他定溶出限制
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-09 DOI: 10.1007/s12247-026-11089-6
Azin Jahangiri, Mahdi Varmazyar, Shahram Emami, Ali Nokhodchi

Purpose

Loratadine, a Biopharmaceutics Classification System (BCS) Class II antihistamine, exhibits dissolution-limited oral delivery due to poor aqueous solubility. This study aimed to develop a hybrid orodispersible tablet (ODT) platform by incorporating a loratadine nanosuspension into a freeze-dried porous matrix to enhance early in vitro dissolution performance.

Methods

A loratadine nanosuspension was prepared using a modified solvent–antisolvent precipitation method combined with high-shear homogenization and characterized for particle size distribution and zeta potential. Conventional ODTs containing raw loratadine and Nano-ODTs incorporating the nanosuspension were prepared using the same mannitol-based freeze-dried matrix. The formulations were evaluated by FTIR, DSC, SEM, disintegration testing, and in vitro dissolution studies.

Results

The pre-lyophilization nanosuspension showed a Z-average diameter of 148.3 nm, PDI of 0.609, and zeta potential of − 26.5 mV. FTIR and DSC analyses indicated compatibility of formulation components and differences in thermal behavior among the formulations. The Nano-ODT exhibited rapid disintegration and higher early loratadine release compared with the conventional ODT under the selected dissolution conditions.

Conclusion

The developed hybrid Nano-ODT platform successfully combined nanosuspension technology with a freeze-dried porous matrix, resulting in improved early in vitro dissolution performance compared with the conventional ODT. These findings support the potential of this approach for improving dissolution-limited delivery of poorly soluble drugs.

目的:氯雷他定是生物制药分类系统(BCS)ⅱ类抗组胺药,由于其水溶性较差,口服给药具有溶出性限制。本研究旨在通过将氯雷他定纳米混悬液掺入冻干多孔基质中,建立一种混合或分散片(ODT)平台,以提高其体外早期溶出性能。方法采用高剪切均质相结合的改进溶剂-抗溶剂沉淀法制备氯雷他定纳米混悬液,并对其粒径分布和zeta电位进行表征。采用相同的甘露醇基冻干基质制备了含有原始氯雷他定的常规odt和含有纳米混悬液的纳米odt。通过FTIR, DSC, SEM,崩解试验和体外溶出度研究对配方进行了评价。结果冻干前纳米悬浮液的z -平均直径为148.3 nm, PDI为0.609,zeta电位为- 26.5 mV。FTIR和DSC分析表明了配方组分的相容性和配方间热行为的差异。在所选择的溶出条件下,与常规ODT相比,纳米ODT崩解速度快,氯雷他定早期释放量高。结论所建立的混合纳米ODT平台成功地将纳米悬浮液技术与冻干多孔基质相结合,与常规ODT相比,其体外早期溶出性能有所提高。这些发现支持了这种方法在改善难溶性药物的溶出限制递送方面的潜力。
{"title":"A Hybrid Nano-ODT Platform: Merging Freeze-Drying and Nanosuspension Technologies to Overcome Loratadine’s Dissolution Limitation","authors":"Azin Jahangiri,&nbsp;Mahdi Varmazyar,&nbsp;Shahram Emami,&nbsp;Ali Nokhodchi","doi":"10.1007/s12247-026-11089-6","DOIUrl":"10.1007/s12247-026-11089-6","url":null,"abstract":"<div><h3>Purpose</h3><p>Loratadine, a Biopharmaceutics Classification System (BCS) Class II antihistamine, exhibits dissolution-limited oral delivery due to poor aqueous solubility. This study aimed to develop a hybrid orodispersible tablet (ODT) platform by incorporating a loratadine nanosuspension into a freeze-dried porous matrix to enhance early in vitro dissolution performance.</p><h3>Methods</h3><p>A loratadine nanosuspension was prepared using a modified solvent–antisolvent precipitation method combined with high-shear homogenization and characterized for particle size distribution and zeta potential. Conventional ODTs containing raw loratadine and Nano-ODTs incorporating the nanosuspension were prepared using the same mannitol-based freeze-dried matrix. The formulations were evaluated by FTIR, DSC, SEM, disintegration testing, and in vitro dissolution studies.</p><h3>Results</h3><p>The pre-lyophilization nanosuspension showed a Z-average diameter of 148.3 nm, PDI of 0.609, and zeta potential of − 26.5 mV. FTIR and DSC analyses indicated compatibility of formulation components and differences in thermal behavior among the formulations. The Nano-ODT exhibited rapid disintegration and higher early loratadine release compared with the conventional ODT under the selected dissolution conditions.</p><h3>Conclusion</h3><p>The developed hybrid Nano-ODT platform successfully combined nanosuspension technology with a freeze-dried porous matrix, resulting in improved early in vitro dissolution performance compared with the conventional ODT. These findings support the potential of this approach for improving dissolution-limited delivery of poorly soluble drugs.</p></div>","PeriodicalId":656,"journal":{"name":"Journal of Pharmaceutical Innovation","volume":"22 1","pages":""},"PeriodicalIF":2.6,"publicationDate":"2026-10-09","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"149132705","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"医学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Multi-component Monitoring of CHO Cell Culture Processes Using Benchtop NMR Spectroscopy Combined with Machine Learning 使用台式核磁共振波谱结合机器学习的CHO细胞培养过程的多组分监测
IF 2.6 4区 医学 Q2 PHARMACOLOGY & PHARMACY Pub Date : 2026-10-09 DOI: 10.1007/s12247-026-11120-w
Yingting Shi, Kerui Fang, Sijun Wu, Yuxiang Wan, Jianyang Pan, Haibin Qu

Purpose

Monitoring of complex bioprocesses is critical for ensuring product quality in biopharmaceutical manufacturing. This study systematically evaluates the potential of benchtop 1H NMR (80 MHz) combined with machine learning as a robust process analytical technology (PAT) tool for bioprocess monitoring.

Methods

A total of 128 samples from eight industrial-scale (1,500 L) CHO-K1 cell culture batches producing Trastuzumab biosimilar were analyzed to acquire both 80 MHz and 600 MHz 1H NMR spectra. Six batches served as training set and two batches as test set. Lasso, Ridge, PLS, and LightGBM models were built with 5-fold cross-validation to predict 36 metabolites, six metal ions, viable cell density (VCD), viability, and antibody titer.

Results

Lasso and PLS models achieved excellent predictions for 36 metabolites (R2 > 0.90, RPD > 3.3) using 80 MHz NMR, comparable to 600 MHz results. Furthermore, our framework enabled the indirect monitoring of indicators that are not directly detectable by 1H NMR under our experimental conditions, including antibody titer, VCD, and metal ions, by leveraging biological correlations. Notably, the 80 MHz Lasso model outperformed its 600 MHz counterpart in predicting antibody titers on the test set (R2 = 0.959), benefiting from reduced data complexity in small-sample modeling. Feature importance analysis revealed that the Lasso models captured chemically meaningful signals aligning with standard metabolite peak positions.

Conclusion

Benchtop NMR coupled with Lasso regression provides a low-cost, information-rich, and interpretable at-line monitoring tool for industrial CHO cell cultures. This approach is particularly advantageous for small-sample scenarios and supports multi-parameter process fingerprinting in biopharmaceutical manufacturing.

目的在生物制药生产过程中,对复杂的生物工艺过程进行监测是保证产品质量的关键。本研究系统地评估了台式1H NMR (80 MHz)结合机器学习作为生物过程监测的强大过程分析技术(PAT)工具的潜力。方法对8批生产曲妥珠单抗生物仿制药的工业规模(1500 L) CHO-K1细胞培养的128个样品进行分析,获得80 MHz和600 MHz的1H NMR谱。6批作为训练集,2批作为测试集。建立Lasso、Ridge、PLS和LightGBM模型,并进行5倍交叉验证,预测36种代谢物、6种金属离子、活细胞密度(VCD)、活力和抗体滴度。结果slasso和PLS模型使用80 MHz NMR对36种代谢物(R2 > 0.90, RPD > 3.3)实现了极好的预测,与600 MHz的结果相当。此外,通过利用生物相关性,我们的框架能够间接监测在我们的实验条件下1H NMR不能直接检测到的指标,包括抗体滴度、VCD和金属离子。值得注意的是,在测试集上,80 MHz Lasso模型在预测抗体滴度方面优于600 MHz模型(R2 = 0.959),这得益于小样本建模降低了数据复杂性。特征重要性分析表明,Lasso模型捕获了与标准代谢物峰位置一致的化学意义信号。结论:台式核磁共振结合Lasso回归为工业CHO细胞培养提供了一种低成本、信息丰富、可解释的在线监测工具。这种方法对于小样本场景特别有利,并支持生物制药制造中的多参数过程指纹识别。
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引用次数: 0
期刊
Journal of Pharmaceutical Innovation
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