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Criminal use of carbamazepine: A case of drug-facilitated captivity in Lubumbashi, DR Congo 卡马西平的犯罪使用:刚果民主共和国卢本巴希的一起毒品促成的囚禁案例
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2025-12-09 DOI: 10.1016/j.fsir.2025.100441
Paul Musa Obadia , Elodie Lwendela Kalasa , Georges Kalenga Ilunga , Tony Kayembe-Kitenge , O. Inès , Margot De Vis , Jan Tytgat , Daniel Okitundu Luwa E-Andjafono , Célestin Banza Lubaba Nkulu , Benoit Nemery
A man was kidnapped and then drugged during a 5-day captivity. After his release, he exhibited various neurological symptoms (inability to walk independently, drowsiness, difficulties to speak, dizziness, headache and a dry mouth). Toxicological analyses of blood and urine samples obtained 3 days after his release revealed therapeutic levels of carbamazepine and its active metabolite in both blood and urine, along with metronidazole and nicotinamide. Carbamazepine has hitherto not been implicated in drug-related crimes. This case highlights the potential misuse of easily available therapeutic drugs for criminal purposes in low-income countries and illustrates the value of prompt international collaboration to elucidate etiologies in forensic toxicology.
一名男子在5天的囚禁中被绑架并下药。释放后,他表现出各种神经系统症状(不能独立行走、嗜睡、说话困难、头晕、头痛和口干)。释放3天后对血液和尿液样本进行毒理学分析,结果显示血液和尿液中卡马西平及其活性代谢物、甲硝唑和烟酰胺均有治疗水平。迄今为止,卡马西平尚未与毒品有关的犯罪有牵连。该案例突出了低收入国家容易获得的治疗药物可能被滥用于犯罪目的,并说明了迅速开展国际合作以阐明法医毒理学病因的价值。
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引用次数: 0
When hoofbeats aren’t always horses: Hepatocellular carcinoma rupture in a Tuberculosis‐Endemic Context 当蹄声不总是马的时候:结核病流行背景下的肝细胞癌破裂
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2026-01-22 DOI: 10.1016/j.fsir.2026.100455
Yasmeen Abdhool, Lienke Perold
Spontaneous rupture of hepatocellular carcinoma (HCC) is an uncommon cause of sudden death, particularly in non-cirrhotic individuals. We report a 59-year-old male who presented with one week of abdominal pain and died unexpectedly. His clinical history included a prior positive GeneXpert test for tuberculosis (2010) and multiple subsequent TB investigations over 15 years, though no record of anti-TB treatment was documented. At autopsy, a massive haemoperitoneum and hepatomegaly were observed, with a focal rupture of the liver capsule. The lungs demonstrated multiple nodules macroscopically suggestive of miliary tuberculosis in a high TB-burden setting. Post-mortem GeneXpert MTB/RIF testing detected Mycobacterium tuberculosis DNA in lung and liver tissue; however, histology revealed no granulomatous inflammation or acid-fast bacilli. Histopathological examination confirmed HCC with regions of both well- and poorly differentiated tumour, vascular invasion, and subcapsular necrosis corresponding to the site of rupture. Pulmonary lesions were consistent with metastatic HCC. This case highlights the diagnostic challenges in high-TB-burden, resource-limited settings, where malignancies may be overlooked due to presumptive attribution of non-specific symptoms to tuberculosis. It underscores the importance of comprehensive differential diagnoses, clinical vigilance, and the value of autopsy in uncovering undiagnosed pathology.
肝细胞癌(HCC)自发性破裂是一种罕见的猝死原因,特别是在非肝硬化个体中。我们报告一个59岁的男性谁提出了一个星期的腹痛和意外死亡。他的临床病史包括先前的结核病GeneXpert检测阳性(2010年)和随后15年的多次结核病调查,但没有记录抗结核治疗的记录。尸检发现大量腹膜出血和肝肿大,肝包膜局灶性破裂。在结核病高负荷环境下,肺部显示多发性结节,提示军旅性结核病。死后GeneXpert MTB/RIF检测在肺和肝组织中检测到结核分枝杆菌DNA;组织学未见肉芽肿性炎症及抗酸杆菌。组织病理学检查证实HCC伴有分化良好和低分化的肿瘤区域、血管浸润和与破裂部位相应的包膜下坏死。肺部病变与转移性HCC一致。该病例突出了结核病高负担和资源有限环境中的诊断挑战,在这些环境中,由于假定将非特异性症状归因于结核病,恶性肿瘤可能被忽视。它强调了综合鉴别诊断的重要性,临床警惕,以及尸检在发现未诊断病理的价值。
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引用次数: 0
Establishing a forensic taphonomy facility at the University of KwaZulu-Natal: Experiences and challenges 在夸祖鲁-纳塔尔省大学建立法医埋藏设施:经验和挑战
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2026-01-20 DOI: 10.1016/j.fsir.2026.100454
Cassandra Creamer , Jolandie Myburgh , Desiré Brits , Brenda Z. De Gama
Forensic taphonomy facilities play an important role in decomposition research by providing controlled environments to investigate decomposition rates, patterns, and the influence of environmental factors on post-mortem interval estimations. Furthermore, establishing such facilities in different geographical locations is important for region-specific research. This paper outlines the experiences and challenges encountered in establishing a forensic taphonomy facility at the University of KwaZulu-Natal, based on guidelines obtained from existing literature. The establishment process involved extensive planning, including securing appropriate land, navigating complex ethical approval processes, obtaining permits, and ensuring compliance with relevant legislation. Financial and security measures also added to the aforementioned challenges. This facility was established with the aim of conducting animal decomposition research to investigate the effects of the humid-subtropical climate on post-mortem interval estimations and to contribute to the broader body of forensic decomposition research in South Africa. The experiences documented in this paper provide insights and guidance for future facility development in South Africa, with the potential to expand access to animal or human decomposition research and training opportunities.
法医埋藏设备在分解研究中发挥着重要的作用,它提供了受控的环境来调查分解速率、模式以及环境因素对死后间隔估计的影响。此外,在不同的地理位置建立这样的设施对于特定区域的研究很重要。本文根据从现有文献中获得的指导方针,概述了在夸祖鲁-纳塔尔省大学建立法医藏药学设施所遇到的经验和挑战。建立过程涉及广泛的规划,包括获得适当的土地,通过复杂的道德审批程序,获得许可证,并确保遵守相关立法。财政和安全措施也增加了上述挑战。建立这个设施的目的是进行动物分解研究,以调查湿润亚热带气候对死后间隔估计的影响,并为南非法医分解研究的更广泛机构作出贡献。本文记录的经验为南非未来的设施发展提供了见解和指导,有可能扩大对动物或人类分解的研究和培训机会。
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引用次数: 0
Chemometric-based machine learning for the forensic classification of fire debris for the presence of self-heating fatty acids following analysis by ASTM E2881 基于化学计量学的机器学习,根据ASTM E2881的分析,对存在自热脂肪酸的火灾碎片进行法医分类
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2025-12-30 DOI: 10.1016/j.fsir.2025.100447
Smith Purdum , Justin P. Miller-Schulze
This work introduces a novel application of chemometric-based preprocessing and machine learning for fire debris analysis, which is crucial in origin and cause investigations. The most technically demanding and interpretative aspect of fire debris analysis is the qualitative classification of GC-MS data using pattern matching, which can be performed by artificial intelligence to support human analysts. Three different methods for preprocessing GC-MS data for machine learning, each requiring varying levels of analyst input, were developed using chromatographic software for feature extraction and data export. These methods were evaluated alongside several machine and deep learning models to classify fire debris and liquid samples containing self-heating fatty acids. The dataset comprised 310 samples (153 positive and 157 negative) generated from spontaneous heating experiments, neat exemplars, forensic casework, and pyrolyzed substrates. Models trained on each preprocessing method were evaluated using repeated 2-fold and Monte Carlo cross-validation across multiple training/testing splits. Within the scope of this data set and preprocessing methods, naive bayes, random forest, and gradient boosting performed best across 2-fold evaluations, with mean accuracies of 100 %, 99.90 %, and 99.65 % for the three preprocessing methods. This pilot study demonstrates a novel, chemometric workflow for fatty acid classification and establishes options for extending machine learning to more complicated fire debris tasks such as ignitable liquid residue analysis. The results imply that machine learning has the potential to enhance fire debris analysis by improving accuracy and analytical efficiency by streamlining routine classification tasks, allowing laboratories to allocate expert effort more effectively and reduce turnaround time.
这项工作介绍了基于化学计量学的预处理和机器学习在火灾碎片分析中的新应用,这在起源和原因调查中至关重要。火灾碎片分析技术要求最高和最具解释性的方面是使用模式匹配对气相色谱-质谱数据进行定性分类,这可以通过人工智能来支持人类分析。使用色谱软件进行特征提取和数据导出,开发了三种不同的用于机器学习的GC-MS数据预处理方法,每种方法都需要不同程度的分析人员输入。这些方法与几种机器和深度学习模型一起进行了评估,以对含有自热脂肪酸的火灾碎片和液体样品进行分类。该数据集包括310个样本(153个阳性和157个阴性),这些样本来自自发加热实验、整齐的范例、法医案例和热解底物。在每个预处理方法上训练的模型在多个训练/测试分割中使用重复的2倍和蒙特卡罗交叉验证进行评估。在该数据集和预处理方法的范围内,朴素贝叶斯、随机森林和梯度增强在2倍评估中表现最好,三种预处理方法的平均准确率分别为100 %、99.90 %和99.65 %。这项初步研究展示了一种新的脂肪酸分类化学计量工作流程,并为将机器学习扩展到更复杂的火灾碎片任务(如可燃液体残留物分析)提供了选择。结果表明,机器学习有可能通过简化常规分类任务来提高准确性和分析效率,从而增强火灾碎片分析,使实验室能够更有效地分配专家工作并缩短周转时间。
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引用次数: 0
DNA barcoding for the identification of swim bladders: An approach to international trade monitoring 鱼鳔DNA条形码鉴定:国际贸易监测的一种方法
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2025-12-05 DOI: 10.1016/j.fsir.2025.100440
Gabriela Idaline de Freitas , Carlos E. Rodrigues Jr , Daniel Eduardo Visciano de Carvalho , Ricardo Utsunomia , Fabio Porto-Foresti
The rapidly expanding global trade in fish maw (dried swim bladders) necessitates urgent forensic monitoring, as this highly processed commodity is morphologically unidentifiable, directly facilitating the illicit inclusion of vulnerable species in the legal supply chain. This research applied DNA Barcoding (cytochrome oxidase I; COI gene) to 120 fish maw samples seized by Brazilian environmental authorities at a major international airport to provide species-level identification and crucial data on trade practices. We identified eight species, with the overwhelming majority belonging to Amazonian Sciaenids (Cynoscion acoupa and Plagioscion auratus) and the catfish Sciades parkeri. Crucially, the definitive identification of C. acoupa and S. parkeri confirms the direct exploitation of species listed as Vulnerable by the IUCN, tracing their flow from multiple Brazilian states to major global consumer hubs, including Hong Kong, the United States, United Kingdom and China. Furthermore, the study exposed a critical methodological constraint: an initial ambiguous species assignment by the BOLD system (94 % match) was only resolved by confirming the correct species, S. parkeri, through the NCBI database (100 % match). This finding demonstrates the essential need for critical evaluation and the utilization of complementary reference libraries to overcome 'code gaps' in forensic analyses. These data underscore the essential role of molecular techniques as an enforcement tool for traceability and provide unequivocal evidence supporting the immediate need for targeted legislation and rigorous regulatory oversight to protect vulnerable Amazonian stocks.
鱼鳔(干鱼鳔)的全球贸易迅速扩大,需要紧急的法医监测,因为这种高度加工的商品在形态上无法识别,直接促进了将脆弱物种非法纳入合法供应链。本研究将DNA条形码(细胞色素氧化酶I; COI基因)应用于巴西环境当局在一个主要国际机场查获的120份鱼鳔样本,以提供物种水平的鉴定和贸易实践的关键数据。我们发现了8种,绝大多数属于亚马逊的Sciaenids (Cynoscion coupa和Plagioscion auratus)和Sciades parkeri鲶鱼。至关重要的是,对coupa和S. parkeri的明确鉴定证实了对IUCN列为易危物种的直接开发,追踪了它们从巴西多个州流向包括香港、美国、英国和中国在内的主要全球消费中心。此外,该研究暴露了一个关键的方法约束:最初由BOLD系统(94 %匹配)进行的模糊物种分配只有通过NCBI数据库(100 %匹配)确认正确的物种parkeri才能解决。这一发现表明了对批判性评估和利用补充参考库来克服法医分析中的“代码缺口”的基本需求。这些数据强调了分子技术作为可追溯性执法工具的重要作用,并提供了明确的证据,支持迫切需要有针对性的立法和严格的监管监督,以保护脆弱的亚马逊种群。
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引用次数: 0
Fatal hemoperitoneum due to rupture of retroperitoneal varices 腹膜后静脉曲张破裂致致命性腹膜出血
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2026-02-03 DOI: 10.1016/j.fsir.2026.100457
Tomoka Yamaguchi, Taiga Nakamura, Shiori Hattori, Keisuke Mizuo, Satoshi Watanabe
A 47-year-old woman was found her sitting on the street. She was a heavy drinker. She went into cardiopulmonary arrest during emergency transport and died in the hospital approximately 45 min after being found. Post-mortem computed tomography (CT) scan showed massive intra-abdominal fluid retention. At autopsy, 2825 mL of blood was found in the intra-abdominal cavity. The liver showed cirrhosis. The source of bleeding was identified as a ruptured varices in the retroperitoneum at the colo–hepatic curvature. Varices may develop as a result of portal hypertension due to cirrhosis, but they generally occur at the gastroesophageal junction. Varices that develop in other locations are referred to as ectopic varices. And among these, retroperitoneal varices are rare. In the present case, the presence of intra-abdominal hemorrhage could be suspected before autopsy based on post-mortem CT findings, but autopsy was necessary to identify the bleeding source. In conclusion, in cases of intra-abdominal hemorrhage in patients with cirrhosis, ectopic variceal rupture should also be considered.
一名47岁的妇女被发现坐在街上。她是个酒鬼。她在紧急运输过程中心肺骤停,被发现后约45 分钟在医院死亡。死后电脑断层扫描显示大量腹内积液。尸检发现腹腔内有2825 mL血液。肝脏显示肝硬化。出血的来源被确定为腹膜后肝弯处静脉曲张破裂。肝硬化引起的门静脉高压可导致静脉曲张,但通常发生在胃食管交界处。在其他部位形成的静脉曲张称为异位静脉曲张。其中,腹膜后静脉曲张是罕见的。在本病例中,根据尸检CT结果,可以在尸检前怀疑腹部出血的存在,但需要尸检来确定出血来源。综上所述,肝硬化患者腹腔内出血时,还应考虑异位静脉曲张破裂。
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引用次数: 0
Single-cell transcriptomics reveals time-resolved neuronal death characteristics in traumatic brain injury 单细胞转录组学揭示了创伤性脑损伤中时间解决的神经元死亡特征
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2026-01-13 DOI: 10.1016/j.fsir.2026.100452
Yang Chen , Manrui Li , Zhuo Li , Xilong Lin , Yang Xu , Shengqiu Qu , Meili Lv , Miao Liao , Lin Zhang , Qiuyun Yang , Xiameng Chen , Weibo Liang
Accurate determination of the timing and progression of traumatic brain injury (TBI) is critical in forensic pathology, particularly for reconstructing injury events and estimating post-traumatic intervals. However, conventional timing approaches of TBI rely on limited pathological features and often lack sufficient accuracy. To address this limitation, we re-analyzed publicly available single-cell RNA-seq datasets from GEO (GSE269748 and GSE160763) and integrated murine cortical transcriptomes across three post-injury stages—acute (24 h), subacute (7 days), and chronic (6 months)—to characterize time-resolved neuronal molecular changes after TBI. Neuron-focused differential expression and functional enrichment analyses revealed a progression from early stress and inflammatory-response programs toward later synaptic and neurodegeneration-associated alterations. We further curated representative gene sets for 14 regulated cell-death programs and quantified their activity using AUCell-derived AUC scoring, identifying stage-dependent shifts in death-associated transcriptional signatures, with higher necroptosis- and pyroptosis-associated signals in the acute phase and increased ferroptosis- and autophagic cell death–associated signals in the chronic phase, accompanied by transcriptional patterns consistent with altered iron handling and glutathione metabolism. This re-analysis provides a time-resolved, neuron-centered molecular framework that may support forensic estimation of injury timing and offers insight into mechanisms of secondary brain injury.
准确确定创伤性脑损伤(TBI)的时间和进展在法医病理学中至关重要,特别是对于重建损伤事件和估计创伤后间隔。然而,传统的TBI定时方法依赖于有限的病理特征,往往缺乏足够的准确性。为了解决这一局限性,我们重新分析了GEO (GSE269748和GSE160763)公开可用的单细胞RNA-seq数据集,并整合了三个损伤后阶段的小鼠皮质转录组——急性(24 h)、亚急性(7天)和慢性(6个月)——以表征TBI后时间分辨的神经元分子变化。神经元集中的差异表达和功能富集分析揭示了从早期应激和炎症反应程序到后期突触和神经变性相关改变的进展。我们进一步整理了14个受调控的细胞死亡程序的代表性基因集,并使用aucell衍生的AUC评分对其活性进行了量化,确定了死亡相关转录特征的阶段依赖性转变,在急性期具有较高的坏死坏死和热死相关信号,在慢性期具有较高的铁坏死和自噬细胞死亡相关信号。伴有与铁处理和谷胱甘肽代谢改变相一致的转录模式。这项重新分析提供了一个时间分辨的、以神经元为中心的分子框架,可以支持损伤时间的法医估计,并为继发性脑损伤的机制提供见解。
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引用次数: 0
Fatal injury from tire explosion during disassembly: A forensic case report 拆轮胎爆炸致人死亡:一份法医案例报告
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2025-12-19 DOI: 10.1016/j.fsir.2025.100445
Shota Furukawa , Ako Sasao , Yuki Ohtsu , Hiroshi Tsutsumi , Chihiro Kawai , Masashi Miyao , Rie Sano , Yoko Nishitani
Cases of fatality caused by a tire explosion are extremely rare, especially during the disassembly process. Tire explosions can occur due to improper techniques during assembly or maintenance; however, serious accidents can also occur during disassembly due to the high-pressure air remaining inside the tire tube, as in this case. We present the case of a man in his 60 s who died after being struck by a tire rim due to a tire explosion during the dismantling of a large wheel and tire set of an airplane passenger boarding bridge. Autopsy revealed complex fractures of the head and chest, fractures of the thoracic vertebrae and upper extremities, and damage to multiple organs. A characteristic feature of this case is thoracic vertebral fracture, which has not been found in previous fatal tire explosion cases, suggesting that the injury resulted from a very large external force. This indicates that discarded tires still contain enough pressurized air to launch the rim, posing a danger equal to or greater than that of tire explosions during assembly or maintenance. This case highlights the importance of safety measures during tire disassembly. Although it is mandatory to use a safety cage to fill the tire with air during maintenance, no such safety measures were undertaken during disassembly. It is necessary to implement safety measures and provide equipment in the workplace to protect the workers.
轮胎爆炸造成死亡的案例极为罕见,特别是在拆卸过程中。在装配或维修过程中,由于技术不当,可能会发生轮胎爆炸;然而,在拆卸过程中,由于高压空气留在轮胎内胎内,也可能发生严重的事故,就像这次一样。我们提出了一个60多岁的男子,他在拆除飞机乘客登机桥的一个大轮子和轮胎组时,因轮胎爆炸而被轮胎圈击中而死亡。尸检显示头部和胸部复杂骨折,胸椎和上肢骨折,多个器官受损。本病例的一个特点是胸椎骨折,这在以往致命的轮胎爆炸病例中没有发现,提示损伤是由非常大的外力造成的。这表明丢弃的轮胎仍然含有足够的加压空气来启动轮辋,造成的危险等于或大于轮胎在组装或维修期间爆炸的危险。这个案例突出了轮胎拆卸过程中安全措施的重要性。虽然在维护过程中必须使用安全笼填充轮胎,但在拆卸过程中没有采取此类安全措施。有必要在工作场所实施安全措施并提供设备来保护工人。
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引用次数: 0
From wrapping to remains: Evaluating eco‑sustainable alternatives to traditional body bags in forensic decomposition studies 从包裹到遗体:在法医分解研究中评估传统尸袋的生态可持续替代品
Q3 Medicine Pub Date : 2026-06-01 DOI: 10.1016/j.fsir.2026.100486
Disha Manjunatha
Accurate interpretation of decomposition is central to forensic investigation, yet the influence of body containment materials remains insufficiently understood. Conventional polyethylene body bags are widely used in forensic and mortuary practice, but interest in more sustainable alternatives is increasing. The forensic consequences of biodegradable wrappings, however, have not been systematically tested within a comparative design. This study examined decomposition under nine conditions using a murine model (n = 27): polyethylene, PLA/PVA bioplastic, linen, cotton, jute, banana leaf, palm leaf, papyrus, and unwrapped controls. Three specimens were allocated to each treatment and deployed for 55 days in a semi-controlled outdoor setting representative of temperate UK summer conditions. Decomposition was assessed morphologically using Total Body Score (TBS) and chemically using surface pH, alongside contextual environmental monitoring. Plastics produced the most rapid early morphological progression, with polyethylene and PLA/PVA reaching TBS 19 by Day 10. Textiles showed steadier trajectories and near-neutral terminal pH values, with linen showing partial desiccation consistent with incipient mummification. Botanical wrappings generated the strongest acidification, with banana leaf and papyrus declining from pH 7.0 at Day 17 to pH 5.0 at Day 55. Exploratory multivariate analysis further suggested clustering by material type. These findings show that wrapping materials create distinct decomposition microenvironments and therefore alter morphological and chemical pathways relevant to post-mortem interval estimation, recovery practice, and the evaluation of sustainable alternatives to polyethylene.
准确解释分解是法医调查的核心,但对尸体收容材料的影响仍未充分了解。传统的聚乙烯尸袋广泛用于法医和太平间的实践,但对更可持续的替代品的兴趣正在增加。然而,可生物降解包装的法医后果尚未在比较设计中进行系统测试。本研究使用小鼠模型(n = 27)检查了九种条件下的分解:聚乙烯、PLA/PVA生物塑料、亚麻、棉花、黄麻、香蕉叶、棕榈叶、纸莎草和未包装的对照。每个处理分配三个标本,并在一个半受控的室外环境中放置55天,代表英国温带夏季条件。利用总体评分(Total Body Score, TBS)进行形态评估,利用表面pH值进行化学评估,同时进行环境监测。塑料的早期形态发展最快,聚乙烯和PLA/PVA在第10天达到TBS 19。纺织品显示出稳定的轨迹和接近中性的终端pH值,亚麻显示出与早期木乃伊化一致的部分干燥。植物膜的酸化作用最强,蕉叶和纸莎草的pH值从第17天的7.0下降到第55天的5.0。探索性多变量分析进一步显示了材料类型的聚类。这些发现表明,包裹材料创造了独特的分解微环境,因此改变了与死后间隔估计、回收实践和可持续聚乙烯替代品评估相关的形态和化学途径。
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引用次数: 0
Proficiency testing of inorganic gunshot residue analysis for laboratory performance assessment 无机枪弹残留物分析实验室性能评估的熟练程度测试
Q3 Medicine Pub Date : 2026-06-01 Epub Date: 2026-05-26 DOI: 10.1016/j.fsir.2026.100485
Worapot Prongmanee , Phuritpach Nantasitangkool , Parinya Seelanan
In forensic examination, inorganic gunshot residue (iGSR) can potentially refer to the act of shooting from a person and become value case evidence. The iGSR analysis is performed by the detection of particles containing antimony (Sb), barium (Ba), or lead (Pb) in a sample. For reliable evidence examination, laboratory competence for the iGSR analysis can be evaluated via the proficiency testing (PT). PT schemes can be achieved by examination of sample magnitude and properties while the iGSR analysis is targeted for quantitative information or characteristic iGSR particles obtained from PT samples. In this study, the Royal Thai Police aims to perform the assessment in comparison with interlaboratory and propose a quick guide to assess the iGSR analysis based on forensic examination techniques, scanning electron microscope with energy dispersive X-ray spectrometer (SEM/EDS) and inductively coupled plasmaoptical emission spectrometry (ICPOES). Standard deviation index (SDI) was employed for the performance assessment. The differences in the interlaboratory results were compared. The nearly zero SDI indicated optimal readiness for both schemes of iGSR analysis. While standard guidelines accept an absolute SDI up to 2, we propose a preliminary internal guideline wherein an absolute SDI above 1 cautiously suggests restricting the laboratory to qualitative-only PT participation. The observed SDI values can be used as a tool for performance assessment and decision making prior to PT subscription of iGSR analysis. Therefore, quick evaluation offers the benefit of time saving and budgets on PT process for each laboratory under the forensic unit in terms of laboratory performance.
在法医鉴定中,无机射击残留物具有潜在的指人的射击行为,成为有价值的案件证据。iGSR分析是通过检测样品中含有锑(Sb)、钡(Ba)或铅(Pb)的颗粒来进行的。为了获得可靠的证据,可以通过能力测试(PT)来评估iGSR分析的实验室能力。PT方案可以通过检查样品的大小和性质来实现,而iGSR分析的目标是从PT样品中获得的定量信息或特征iGSR颗粒。在本研究中,泰国皇家警察旨在与实验室间进行比较评估,并提出基于法医检验技术,扫描电子显微镜与能量色散x射线光谱仪(SEM/EDS)和电感耦合等离子体光学发射光谱(ICPOES)的iGSR分析评估快速指南。采用标准偏差指数(SDI)进行绩效评价。比较了实验室间结果的差异。几乎为零的SDI表明两种iGSR分析方案的最佳准备。虽然标准指南接受绝对SDI不超过2,但我们提出了一个初步的内部指南,其中绝对SDI高于1谨慎地建议限制实验室只参与定性PT。观测到的SDI值可以作为iGSR分析PT订阅前的绩效评估和决策工具。因此,快速评估为法医单位下的每个实验室在实验室绩效方面节省了时间和预算。
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引用次数: 0
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Forensic Science International: Reports
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